Crystal system: triclinic
| a: | 12.2981 Å |
| b: | 12.3163 Å |
| c: | 17.2102 Å |
| α: | 83.575° |
| β: | 79.708° |
| γ: | 89.976° |
Starting materials: n-Butanol, 57wt% stabilized HI (Alfa Aesar), perfluorophenethylammonium iodide (F5-PEAI; synthesized), phenethylammonium iodide (PEAI; synthesized)
Product: Yellow plate-like crystals
Description: In 0.5 ml n-Butanol and 0.1 ml 57wt% stabilized HI, 69.2 mg PbI2, 50.9 mg F5-PEAI and 37.4 mg PEAI were dissolved at 95 °C. The solution was slowly cooled down at 1 °C/h to room temperature and the solids were collected.
Method: Single crystal X-ray Diffraction
Description: Bruker D8 Quest ECO diffractometer equipped with a microfocus Mo K radiation source and Photon 50 CMOS half-plate detector was used for SCXRD data collection at room temperature.