Crystal system: monoclinic
| a: | 12.4 (±0.003) Å |
| b: | 7.8407 (±0.0019) Å |
| c: | 8.385 (±0.002) Å |
| α: | 90° |
| β: | 108.177 (±0.004)° |
| γ: | 90° |
Starting materials: PbBr2, HBr, C3H5NH2
Product: Colorless crystals
Description: PbBr2 was dissolved in an HBr solution. Then, the cyclic amine was added and immediately resulted in the precipitation of a solid, which was re-dissolved by refluxing for 1-12 hours. The solution was then cooled slowly to room temperature, causing crystals to precipitate.
Method: Single-crystal X-ray diffraction
Description: A Bruker SMART 1K CCD area detector diffractometer using Mo Kalpha radiation was used to collect the SCXRD data. Omega-scans of width 0.3 degrees were used. The SAINT+ program, version 6.02, was used to perform data reduction and the XPREP program was used to perform face indexed absorption corrections. The SHELXS-97 program was used for solving the structure, and the SHELXL-97 program was used to refine it by full matrix least-squares minimization.
Crystal system: monoclinic
| a: | 13.278 (±0.003) Å |
| b: | 7.9463 (±0.0018) Å |
| c: | 8.4703 (±0.0019) Å |
| α: | 90° |
| β: | 108.43 (±0.004)° |
| γ: | 90° |
Starting materials: PbBr2, HBr, C4H7NH2
Product: Colorless crystals
Description: PbBr2 was dissolved in an HBr solution. Then, the cyclic amine was added and immediately resulted in the precipitation of a solid, which was re-dissolved by refluxing for 1-12 hours. The solution was then cooled slowly to room temperature, causing crystals to precipitate.
Method: Single-crystal X-ray diffraction
Description: A Bruker SMART 1K CCD area detector diffractometer using Mo Kalpha radiation was used to collect the SCXRD data. Omega-scans of width 0.3 degrees were used. The SAINT+ program, version 6.02, was used to perform data reduction and the XPREP program was used to perform face indexed absorption corrections. The SHELXS-97 program was used for solving the structure, and the SHELXL-97 program was used to refine it by full matrix least-squares minimization.
Crystal system: monoclinic
| a: | 13.429 (±0.003) Å |
| b: | 7.9862 (±0.0019) Å |
| c: | 8.8 (±0.002) Å |
| α: | 90° |
| β: | 106.163 (±0.004)° |
| γ: | 90° |
Starting materials: PbBr2, HBr, C5H9NH2
Product: Colorless crystals
Description: PbBr2 was dissolved in an HBr solution. Then, the cyclic amine was added and immediately resulted in the precipitation of a solid, which was re-dissolved by refluxing for 1-12 hours. The solution was then cooled slowly to room temperature, causing crystals to precipitate.
Method: Single-crystal X-ray diffraction
Description: A Bruker SMART 1K CCD area detector diffractometer using Mo Kalpha radiation was used to collect the SCXRD data. Omega-scans of width 0.3 degrees were used. The SAINT+ program, version 6.02, was used to perform data reduction and the XPREP program was used to perform face indexed absorption corrections. The SHELXS-97 program was used for solving the structure, and the SHELXL-97 program was used to refine it by full matrix least-squares minimization.
See all entries for this property (3 total)
Crystal system: orthorhombic
| a: | 27.788 (±0.005) Å |
| b: | 8.6541 (±0.0014) Å |
| c: | 8.2367 (±0.0013) Å |
| α: | 90° |
| β: | 90° |
| γ: | 90° |
Starting materials: PbBr2, HBr, C6H11NH2
Product: Orange crystals
Description: PbBr2 was dissolved in an HBr solution. Then, the cyclic amine was added and immediately resulted in the precipitation of a solid, which was re-dissolved by refluxing for 1-12 hours. The solution was then cooled slowly to room temperature, causing crystals to precipitate.
Method: Single-crystal X-ray diffraction
Description: A Bruker SMART 1K CCD area detector diffractometer using Mo Kalpha radiation was used to collect the SCXRD data. Omega-scans of width 0.3 degrees were used. The SAINT+ program, version 6.02, was used to perform data reduction and the XPREP program was used to perform face indexed absorption corrections. The SHELXS-97 program was used for solving the structure, and the SHELXL-97 program was used to refine it by full matrix least-squares minimization.
Crystal system: orthorhombic
| a: | 8.0888 (±0.0004) Å |
| b: | 27.1707 (±0.0015) Å |
| c: | 28.9932 (±0.0016) Å |
| α: | 90° |
| β: | 90° |
| γ: | 90° |
Starting materials: PbBr2, HBr, C7H13NH2
Product: Colorless crystals
Description: PbBr2 was dissolved in an HBr solution. Then, the cyclic amine was added and immediately resulted in the precipitation of a solid, which was re-dissolved by refluxing for 1-12 hours. The solution was then cooled slowly to room temperature, causing crystals to precipitate.
Method: Single-crystal X-ray diffraction
Description: A Bruker SMART 1K CCD area detector diffractometer using Mo Kalpha radiation was used to collect the SCXRD data. Omega-scans of width 0.3 degrees were used. The SAINT+ program, version 6.02, was used to perform data reduction and the XPREP program was used to perform face indexed absorption corrections. The SHELXS-97 program was used for solving the structure, and the SHELXL-97 program was used to refine it by full matrix least-squares minimization.
Crystal system: triclinic
| a: | 11.7861 (±0.0011) Å |
| b: | 16.0354 (±0.0016) Å |
| c: | 31.135 (±0.003) Å |
| α: | 92.891 (±0.004)° |
| β: | 96.42 (±0.004)° |
| γ: | 100.267 (±0.004)° |
Starting materials: PbBr2, HBr, C8H15NH2
Product: Colorless crystals
Description: PbBr2 was dissolved in an HBr solution. Then, the cyclic amine was added and immediately resulted in the precipitation of a solid, which was re-dissolved by refluxing for 1-12 hours. The solution was then cooled slowly to room temperature, causing crystals to precipitate.
Method: Single-crystal X-ray diffraction
Description: A Bruker SMART 1K CCD area detector diffractometer using Mo Kalpha radiation was used to collect the SCXRD data. Omega-scans of width 0.3 degrees were used. The SAINT+ program, version 6.02, was used to perform data reduction and the XPREP program was used to perform face indexed absorption corrections. The SHELXS-97 program was used for solving the structure, and the SHELXL-97 program was used to refine it by full matrix least-squares minimization.
Crystal system: monoclinic
| a: | 12.187 (±0.005) Å |
| b: | 7.508 (±0.003) Å |
| c: | 8.054 (±0.003) Å |
| α: | 90° |
| β: | 109.141 (±0.006)° |
| γ: | 90° |
Starting materials: PbCl2, HCl, C3H5NH2
Product: Colorless crystals
Description: PbCl2 was dissolved in an HCl solution. Then, the cyclic amine was added and immediately resulted in the precipitation of a solid, which was re-dissolved by refluxing for 1-12 hours. The solution was then cooled slowly to room temperature, causing crystals to precipitate.
Method: Single-crystal X-ray diffraction
Description: A Bruker SMART 1K CCD area detector diffractometer using Mo Kalpha radiation was used to collect the SCXRD data. Omega-scans of width 0.3 degrees were used. The SAINT+ program, version 6.02, was used to perform data reduction and the XPREP program was used to perform face indexed absorption corrections. The SHELXS-97 program was used for solving the structure, and the SHELXL-97 program was used to refine it by full matrix least-squares minimization.
Crystal system: monoclinic
| a: | 13.219 (±0.005) Å |
| b: | 7.618 (±0.003) Å |
| c: | 8.093 (±0.003) Å |
| α: | 90° |
| β: | 106.828 (±0.007)° |
| γ: | 90° |
Starting materials: PbCl2, HCl, C4H7NH2
Product: Colorless crystals
Description: PbCl2 was dissolved in an HCl solution. Then, the cyclic amine was added and immediately resulted in the precipitation of a solid, which was re-dissolved by refluxing for 1-12 hours. The solution was then cooled slowly to room temperature, causing crystals to precipitate.
Method: Single-crystal X-ray diffraction
Description: A Bruker SMART 1K CCD area detector diffractometer using Mo Kalpha radiation was used to collect the SCXRD data. Omega-scans of width 0.3 degrees were used. The SAINT+ program, version 6.02, was used to perform data reduction and the XPREP program was used to perform face indexed absorption corrections. The SHELXS-97 program was used for solving the structure, and the SHELXL-97 program was used to refine it by full matrix least-squares minimization.
Crystal system: orthorhombic
| a: | 25.842 (±0.001) Å |
| b: | 8.5174 (±0.0003) Å |
| c: | 7.6956 (±0.0003) Å |
| α: | 90° |
| β: | 90° |
| γ: | 90° |
Starting materials: PbCl2, HCl, C5H9NH2
Product: Colorless crystals
Description: PbCl2 was dissolved in an HCl solution. Then, the cyclic amine was added and immediately resulted in the precipitation of a solid, which was re-dissolved by refluxing for 1-12 hours. The solution was then cooled slowly to room temperature, causing crystals to precipitate.
Method: Single-crystal X-ray diffraction
Description: A Bruker SMART 1K CCD area detector diffractometer using Mo Kalpha radiation was used to collect the SCXRD data. Omega-scans of width 0.3 degrees were used. The SAINT+ program, version 6.02, was used to perform data reduction and the XPREP program was used to perform face indexed absorption corrections. The SHELXS-97 program was used for solving the structure, and the SHELXL-97 program was used to refine it by full matrix least-squares minimization.
Crystal system: monoclinic
| a: | 11.4446 (±0.0011) Å |
| b: | 28.306 (±0.003) Å |
| c: | 11.5206 (±0.001) Å |
| α: | 90° |
| β: | 90.031 (±0.006)° |
| γ: | 90° |
Starting materials: PbCl2, HCl, C6H11NH2
Product: Colorless crystals
Description: PbCl2 was dissolved in an HCl solution. Then, the cyclic amine was added and immediately resulted in the precipitation of a solid, which was re-dissolved by refluxing for 1-12 hours. The solution was then cooled slowly to room temperature, causing crystals to precipitate.
Method: Single-crystal X-ray diffraction
Description: A Bruker SMART 1K CCD area detector diffractometer using Mo Kalpha radiation was used to collect the SCXRD data. Omega-scans of width 0.3 degrees were used. The SAINT+ program, version 6.02, was used to perform data reduction and the XPREP program was used to perform face indexed absorption corrections. The SHELXS-97 program was used for solving the structure, and the SHELXL-97 program was used to refine it by full matrix least-squares minimization.
Crystal system: monoclinic
| a: | 12.7667 (±0.0015) Å |
| b: | 46.043 (±0.005) Å |
| c: | 14.9592 (±0.0015) Å |
| α: | 90° |
| β: | 94.385 (±0.005)° |
| γ: | 90° |
Starting materials: PbCl2, HCl, C7H13NH2
Product: Colorless crystals
Description: PbCl2 was dissolved in an HCl solution. Then, the cyclic amine was added and immediately resulted in the precipitation of a solid, which was re-dissolved by refluxing for 1-12 hours. The solution was then cooled slowly to room temperature, causing crystals to precipitate.
Method: Single-crystal X-ray diffraction
Description: A Bruker SMART 1K CCD area detector diffractometer using Mo Kalpha radiation was used to collect the SCXRD data. Omega-scans of width 0.3 degrees were used. The SAINT+ program, version 6.02, was used to perform data reduction and the XPREP program was used to perform face indexed absorption corrections. The SHELXS-97 program was used for solving the structure, and the SHELXL-97 program was used to refine it by full matrix least-squares minimization.
Crystal system: triclinic
| a: | 17.365 (±0.003) Å |
| b: | 19.016 (±0.004) Å |
| c: | 19.357 (±0.004) Å |
| α: | 63.476 (±0.003)° |
| β: | 70.493 (±0.004)° |
| γ: | 88.146 (±0.004)° |
Starting materials: PbCl2, HCl, C8H15NH2
Product: Colorless crystals
Description: PbCl2 was dissolved in an HCl solution. Then, the cyclic amine was added and immediately resulted in the precipitation of a solid, which was re-dissolved by refluxing for 1-12 hours. The solution was then cooled slowly to room temperature, causing crystals to precipitate.
Method: Single-crystal X-ray diffraction
Description: A Bruker SMART 1K CCD area detector diffractometer using Mo Kalpha radiation was used to collect the SCXRD data. Omega-scans of width 0.3 degrees were used. The SAINT+ program, version 6.02, was used to perform data reduction and the XPREP program was used to perform face indexed absorption corrections. The SHELXS-97 program was used for solving the structure, and the SHELXL-97 program was used to refine it by full matrix least-squares minimization.