See all entries for this property (24 total)
Crystal system: orthorhombic
| a: | 7.9814 Å |
| b: | 11.8623 Å |
| c: | 8.5846 Å |
| α: | 90° |
| β: | 90° |
| γ: | 90° |
Starting materials: 1M solution of PbBr2 and CH3NH3Br in dimethylformamide (DMF)
Product: CH3 NH3 PbBr3 crystals
Description: 1M solution of PbBr2 and CH3NH3Br in DMF passed through 0.22 micron filter, filtered solution heated in oil bath to 82 degrees C, removed after 30 minutes. CH3 NH3 PbBr3 crystals form and are isolated quickly from the remaining liquid to avoid redissolution.
Method: Single crystal X-ray diffraction
Description: Performed using a Bruker D8 venture diffractometer with Photon 100 CMOS detector. Oxford Cryostream for temperature control. Mo K-alpha radiation (0.71703 Angstrom) was used. phi and omega angle scans were performed, frames integrated and absorption correction performed (implemented in Bruker APEX 3 software). Structure was solved using SHELXT software and refined (Olex 2 software package). Pb and Br thermal displacement parameters refined anisotropically; C, N, and H parameters are refined isotropically. The C-N bond length was constrained to 1.47 Angstroms.
See all entries for this property (24 total)
Crystal system: orthorhombic
| a: | 8.0034 Å |
| b: | 11.8622 Å |
| c: | 8.5727 Å |
| α: | 90° |
| β: | 90° |
| γ: | 90° |
Starting materials: 1M solution of PbBr2 and CH3NH3Br in dimethylformamide (DMF)
Product: CH3 NH3 PbBr3 crystals
Description: 1M solution of PbBr2 and CH3NH3Br in DMF passed through 0.22 micron filter, filtered solution heated in oil bath to 82 degrees C, removed after 30 minutes. CH3 NH3 PbBr3 crystals form and are isolated quickly from the remaining liquid to avoid redissolution.
Method: Single crystal X-ray diffraction
Description: Performed using a Bruker D8 venture diffractometer with Photon 100 CMOS detector. Oxford Cryostream for temperature control. Mo K-alpha radiation (0.71703 Angstrom) was used. phi and omega angle scans were performed, frames integrated and absorption correction performed (implemented in Bruker APEX 3 software). Structure was solved using SHELXT software and refined (Olex 2 software package). Pb and Br thermal displacement parameters refined anisotropically; C, N, and H parameters are refined isotropically. The C-N bond length was constrained to 1.47 Angstroms.
See all entries for this property (24 total)
Crystal system: orthorhombic
| a: | 8.0257 Å |
| b: | 11.869 Å |
| c: | 8.5693 Å |
| α: | 90° |
| β: | 90° |
| γ: | 90° |
Starting materials: 1M solution of PbBr2 and CH3NH3Br in dimethylformamide (DMF)
Product: CH3 NH3 PbBr3 crystals
Description: 1M solution of PbBr2 and CH3NH3Br in DMF passed through 0.22 micron filter, filtered solution heated in oil bath to 82 degrees C, removed after 30 minutes. CH3 NH3 PbBr3 crystals form and are isolated quickly from the remaining liquid to avoid redissolution.
Method: Single crystal X-ray diffraction
Description: Performed using a Bruker D8 venture diffractometer with Photon 100 CMOS detector. Oxford Cryostream for temperature control. Mo K-alpha radiation (0.71703 Angstrom) was used. phi and omega angle scans were performed, frames integrated and absorption correction performed (implemented in Bruker APEX 3 software). Structure was solved using SHELXT software and refined (Olex 2 software package). Pb and Br thermal displacement parameters refined anisotropically; C, N, and H parameters are refined isotropically. The C-N bond length was constrained to 1.47 Angstroms.
See all entries for this property (24 total)
Crystal system: tetragonal
| a: | 8.3143 Å |
| b: | 8.3143 Å |
| c: | 11.877 Å |
| α: | 90° |
| β: | 90° |
| γ: | 90° |
Starting materials: 1M solution of PbBr2 and CH3NH3Br in dimethylformamide (DMF)
Product: CH3 NH3 PbBr3 crystals
Description: 1M solution of PbBr2 and CH3NH3Br in DMF passed through 0.22 micron filter, filtered solution heated in oil bath to 82 degrees C, removed after 30 minutes. CH3 NH3 PbBr3 crystals form and are isolated quickly from the remaining liquid to avoid redissolution.
Method: Single crystal X-ray diffraction
Description: Performed using a Bruker D8 venture diffractometer with Photon 100 CMOS detector. Oxford Cryostream for temperature control. Mo K-alpha radiation (0.71703 Angstrom) was used. phi and omega angle scans were performed, frames integrated and absorption correction performed (implemented in Bruker APEX 3 software). Structure was solved using SHELXT software and refined (Olex 2 software package). Pb and Br thermal displacement parameters refined anisotropically; C, N, and H parameters are refined isotropically. The C-N bond length was constrained to 1.47 Angstroms.
See all entries for this property (24 total)
Crystal system: tetragonal
| a: | 8.3179 Å |
| b: | 8.3179 Å |
| c: | 11.881 Å |
| α: | 90° |
| β: | 90° |
| γ: | 90° |
Starting materials: 1M solution of PbBr2 and CH3NH3Br in dimethylformamide (DMF)
Product: CH3 NH3 PbBr3 crystals
Description: 1M solution of PbBr2 and CH3NH3Br in DMF passed through 0.22 micron filter, filtered solution heated in oil bath to 82 degrees C, removed after 30 minutes. CH3 NH3 PbBr3 crystals form and are isolated quickly from the remaining liquid to avoid redissolution.
Method: Single crystal X-ray diffraction
Description: Performed using a Bruker D8 venture diffractometer with Photon 100 CMOS detector. Oxford Cryostream for temperature control. Mo K-alpha radiation (0.71703 Angstrom) was used. phi and omega angle scans were performed, frames integrated and absorption correction performed (implemented in Bruker APEX 3 software). Structure was solved using SHELXT software and refined (Olex 2 software package). Pb and Br thermal displacement parameters refined anisotropically; C, N, and H parameters are refined isotropically. The C-N bond length was constrained to 1.47 Angstroms.
See all entries for this property (24 total)
Crystal system: tetragonal
| a: | 8.3315 Å |
| b: | 8.3315 Å |
| c: | 11.8751 Å |
| α: | 90° |
| β: | 90° |
| γ: | 90° |
Starting materials: 1M solution of PbBr2 and CH3NH3Br in dimethylformamide (DMF)
Product: CH3 NH3 PbBr3 crystals
Description: 1M solution of PbBr2 and CH3NH3Br in DMF passed through 0.22 micron filter, filtered solution heated in oil bath to 82 degrees C, removed after 30 minutes. CH3 NH3 PbBr3 crystals form and are isolated quickly from the remaining liquid to avoid redissolution.
Method: Single crystal X-ray diffraction
Description: Performed using a Bruker D8 venture diffractometer with Photon 100 CMOS detector. Oxford Cryostream for temperature control. Mo K-alpha radiation (0.71703 Angstrom) was used. phi and omega angle scans were performed, frames integrated and absorption correction performed (implemented in Bruker APEX 3 software). Structure was solved using SHELXT software and refined (Olex 2 software package). Pb and Br thermal displacement parameters refined anisotropically; C, N, and H parameters are refined isotropically. The C-N bond length was constrained to 1.47 Angstroms.
See all entries for this property (24 total)
Crystal system: tetragonal
| a: | 8.347 Å |
| b: | 8.347 Å |
| c: | 11.8604 Å |
| α: | 90° |
| β: | 90° |
| γ: | 90° |
Starting materials: 1M solution of PbBr2 and CH3NH3Br in dimethylformamide (DMF)
Product: CH3 NH3 PbBr3 crystals
Description: 1M solution of PbBr2 and CH3NH3Br in DMF passed through 0.22 micron filter, filtered solution heated in oil bath to 82 degrees C, removed after 30 minutes. CH3 NH3 PbBr3 crystals form and are isolated quickly from the remaining liquid to avoid redissolution.
Method: Single crystal X-ray diffraction
Description: Performed using a Bruker D8 venture diffractometer with Photon 100 CMOS detector. Oxford Cryostream for temperature control. Mo K-alpha radiation (0.71703 Angstrom) was used. phi and omega angle scans were performed, frames integrated and absorption correction performed (implemented in Bruker APEX 3 software). Structure was solved using SHELXT software and refined (Olex 2 software package). Pb and Br thermal displacement parameters refined anisotropically; C, N, and H parameters are refined isotropically. The C-N bond length was constrained to 1.47 Angstroms.
See all entries for this property (24 total)
Crystal system: tetragonal
| a: | 8.3555 Å |
| b: | 8.3555 Å |
| c: | 11.8514 Å |
| α: | 90° |
| β: | 90° |
| γ: | 90° |
Starting materials: 1M solution of PbBr2 and CH3NH3Br in dimethylformamide (DMF)
Product: CH3 NH3 PbBr3 crystals
Description: 1M solution of PbBr2 and CH3NH3Br in DMF passed through 0.22 micron filter, filtered solution heated in oil bath to 82 degrees C, removed after 30 minutes. CH3 NH3 PbBr3 crystals form and are isolated quickly from the remaining liquid to avoid redissolution.
Method: Single crystal X-ray diffraction
Description: Performed using a Bruker D8 venture diffractometer with Photon 100 CMOS detector. Oxford Cryostream for temperature control. Mo K-alpha radiation (0.71703 Angstrom) was used. phi and omega angle scans were performed, frames integrated and absorption correction performed (implemented in Bruker APEX 3 software). Structure was solved using SHELXT software and refined (Olex 2 software package). Pb and Br thermal displacement parameters refined anisotropically; C, N, and H parameters are refined isotropically. The C-N bond length was constrained to 1.47 Angstroms.
See all entries for this property (24 total)
Crystal system: cubic
| a: | 5.9162 Å |
| b: | 5.9162 Å |
| c: | 5.9162 Å |
| α: | 90° |
| β: | 90° |
| γ: | 90° |
Starting materials: 1M solution of PbBr2 and CH3NH3Br in dimethylformamide (DMF)
Product: CH3 NH3 PbBr3 crystals
Description: 1M solution of PbBr2 and CH3NH3Br in DMF passed through 0.22 micron filter, filtered solution heated in oil bath to 82 degrees C, removed after 30 minutes. CH3 NH3 PbBr3 crystals form and are isolated quickly from the remaining liquid to avoid redissolution.
Method: Single crystal X-ray diffraction
Description: Performed using a Bruker D8 venture diffractometer with Photon 100 CMOS detector. Oxford Cryostream for temperature control. Mo K-alpha radiation (0.71703 Angstrom) was used. phi and omega angle scans were performed, frames integrated and absorption correction performed (implemented in Bruker APEX 3 software). Structure was solved using SHELXT software and refined (Olex 2 software package). Pb and Br thermal displacement parameters refined anisotropically; C, N, and H parameters are refined isotropically. The C-N bond length was constrained to 1.47 Angstroms.
See all entries for this property (24 total)
Crystal system: cubic
| a: | 5.9183 Å |
| b: | 5.9183 Å |
| c: | 5.9183 Å |
| α: | 90° |
| β: | 90° |
| γ: | 90° |
Starting materials: 1M solution of PbBr2 and CH3NH3Br in dimethylformamide (DMF)
Product: CH3 NH3 PbBr3 crystals
Description: 1M solution of PbBr2 and CH3NH3Br in DMF passed through 0.22 micron filter, filtered solution heated in oil bath to 82 degrees C, removed after 30 minutes. CH3 NH3 PbBr3 crystals form and are isolated quickly from the remaining liquid to avoid redissolution.
Method: Single crystal X-ray diffraction
Description: Performed using a Bruker D8 venture diffractometer with Photon 100 CMOS detector. Oxford Cryostream for temperature control. Mo K-alpha radiation (0.71703 Angstrom) was used. phi and omega angle scans were performed, frames integrated and absorption correction performed (implemented in Bruker APEX 3 software). Structure was solved using SHELXT software and refined (Olex 2 software package). Pb and Br thermal displacement parameters refined anisotropically; C, N, and H parameters are refined isotropically. The C-N bond length was constrained to 1.47 Angstroms.
See all entries for this property (24 total)
Crystal system: cubic
| a: | 5.9204 Å |
| b: | 5.9204 Å |
| c: | 5.9204 Å |
| α: | 90° |
| β: | 90° |
| γ: | 90° |
Starting materials: 1M solution of PbBr2 and CH3NH3Br in dimethylformamide (DMF)
Product: CH3 NH3 PbBr3 crystals
Description: 1M solution of PbBr2 and CH3NH3Br in DMF passed through 0.22 micron filter, filtered solution heated in oil bath to 82 degrees C, removed after 30 minutes. CH3 NH3 PbBr3 crystals form and are isolated quickly from the remaining liquid to avoid redissolution.
Method: Single crystal X-ray diffraction
Description: Performed using a Bruker D8 venture diffractometer with Photon 100 CMOS detector. Oxford Cryostream for temperature control. Mo K-alpha radiation (0.71703 Angstrom) was used. phi and omega angle scans were performed, frames integrated and absorption correction performed (implemented in Bruker APEX 3 software). Structure was solved using SHELXT software and refined (Olex 2 software package). Pb and Br thermal displacement parameters refined anisotropically; C, N, and H parameters are refined isotropically. The C-N bond length was constrained to 1.47 Angstroms.
See all entries for this property (24 total)
Crystal system: cubic
| a: | 5.9246 Å |
| b: | 5.9246 Å |
| c: | 5.9246 Å |
| α: | 90° |
| β: | 90° |
| γ: | 90° |
Starting materials: 1M solution of PbBr2 and CH3NH3Br in dimethylformamide (DMF)
Product: CH3 NH3 PbBr3 crystals
Description: 1M solution of PbBr2 and CH3NH3Br in DMF passed through 0.22 micron filter, filtered solution heated in oil bath to 82 degrees C, removed after 30 minutes. CH3 NH3 PbBr3 crystals form and are isolated quickly from the remaining liquid to avoid redissolution.
Method: Single crystal X-ray diffraction
Description: Performed using a Bruker D8 venture diffractometer with Photon 100 CMOS detector. Oxford Cryostream for temperature control. Mo K-alpha radiation (0.71703 Angstrom) was used. phi and omega angle scans were performed, frames integrated and absorption correction performed (implemented in Bruker APEX 3 software). Structure was solved using SHELXT software and refined (Olex 2 software package). Pb and Br thermal displacement parameters refined anisotropically; C, N, and H parameters are refined isotropically. The C-N bond length was constrained to 1.47 Angstroms.
See all entries for this property (24 total)
Crystal system: cubic
| a: | 5.9287 Å |
| b: | 5.9287 Å |
| c: | 5.9287 Å |
| α: | 90° |
| β: | 90° |
| γ: | 90° |
Starting materials: 1M solution of PbBr2 and CH3NH3Br in dimethylformamide (DMF)
Product: CH3 NH3 PbBr3 crystals
Description: 1M solution of PbBr2 and CH3NH3Br in DMF passed through 0.22 micron filter, filtered solution heated in oil bath to 82 degrees C, removed after 30 minutes. CH3 NH3 PbBr3 crystals form and are isolated quickly from the remaining liquid to avoid redissolution.
Method: Single crystal X-ray diffraction
Description: Performed using a Bruker D8 venture diffractometer with Photon 100 CMOS detector. Oxford Cryostream for temperature control. Mo K-alpha radiation (0.71703 Angstrom) was used. phi and omega angle scans were performed, frames integrated and absorption correction performed (implemented in Bruker APEX 3 software). Structure was solved using SHELXT software and refined (Olex 2 software package). Pb and Br thermal displacement parameters refined anisotropically; C, N, and H parameters are refined isotropically. The C-N bond length was constrained to 1.47 Angstroms.