Crystal system: monoclinic
| a: | 7.7688 (±0.0003) Å |
| b: | 8.5108 (±0.0004) Å |
| c: | 24.6314 (±0.0011) Å |
| α: | 90° |
| β: | 95.197 (±0.002)° |
| γ: | 90° |
Starting materials: 3-(2-ammonioethyl)anilin, PbBr2, HBr
Product: plate-like colorless crystals
Description: 0.34 mmol PbBr2, 0.35 mmol 3-(2-ammonioethyl)anilin are mixed in 3 mL of 9M HBr. The mixture is then heated to 100 ˚C for 2 h to dissolve the solid, and then slowly cooled down to room temperature at −2 °C·hr−1.
Method: Single crystal X-ray diffraction
Description: Frames were collected using Bruker D85 diffractometer at the Advanced Light Source beamline 11.3.1 (λ=0.7749 Å).