Crystal system: monoclinic
| a: | 24.4632 (±0.0015) Å |
| b: | 8.0039 (±0.0004) Å |
| c: | 8.1963 (±0.0005) Å |
| α: | 90° |
| β: | 99.745 (±0.002)° |
| γ: | 90° |
Starting materials: 2-methyl-1,5-pentanediamine, PbBr2, HBr
Product: needle-like colorless crystal
Description: 0.34 mmol PbBr2, 0.35 mmol 2-methyl-1,5-pentanediamine are mixed in 3 mL of 9M HBr. The mixture is then heated to 100 ˚C for 2 h to dissolve the solid, and then slowly cooled down to room temperature at −2 °C·hr−1.
Method: Single crystal X-ray diffraction
Description: Frames were collected using Bruker D8 Venture diffractometer equipped with a Photon 100 CMOS detector employing Mo Kα radiation (λ=0.71073 Å).
See all entries for this property (2 total)
Crystal system: orthorhombic
| a: | 8.3343 (±0.0003) Å |
| b: | 8.2225 (±0.0004) Å |
| c: | 27.6171 (±0.0015) Å |
| α: | 90° |
| β: | 90° |
| γ: | 90° |
Starting materials: n-butylamine, PbBr2, HBr
Product: plate-like colorless crystals
Description: 0.34 mmol PbBr2, 0.7 mmol n-butylamine are mixed in 3 mL of 9M HBr. The mixture is then heated to 100 ˚C for 2 h to dissolve the solid, and then slowly cooled down to room temperature at −2 °C·hr−1.
Method: Single crystal X-ray diffraction
Description: Frames were collected using Bruker D8 Venture diffractometer equipped with a Photon 100 CMOS detector employing Mo Kα radiation (λ=0.71073 Å).
Crystal system: monoclinic
| a: | 13.807 (±0.003) Å |
| b: | 7.9891 (±0.0014) Å |
| c: | 8.2769 (±0.0014) Å |
| α: | 90° |
| β: | 104.34 (±0.006)° |
| γ: | 90° |
Starting materials: octanediamine, PbBr2, HBr
Product: plate-like colorless crystals
Description: 0.34 mmol PbBr2, 0.35 mmol octanediamine are mixed in 3 mL of 9M HBr. The mixture is then heated to 100 ˚C for 2 h to dissolve the solid, and then slowly cooled down to room temperature at −2 °C·hr−1.
Method: Single crystal X-ray diffraction
Description: Frames were collected using Bruker D8 Venture diffractometer equipped with a Photon 100 CMOS detector employing Mo Kα radiation (λ=0.71073 Å).
Crystal system: monoclinic
| a: | 24.7721 (±0.0012) Å |
| b: | 8.0709 (±0.0004) Å |
| c: | 56.964 (±0.003) Å |
| α: | 90° |
| β: | 97.137 (±0.002)° |
| γ: | 90° |
Starting materials: 3-carboxypropan-1-amine, PbBr2, HBr
Product: plate-like colorless crystals
Description: 0.34 mmol PbBr2, 0.7 mmol 3-carboxypropan-1-amine are mixed in 3 mL of 9M HBr. The mixture is then heated to 100 ˚C for 2 h to dissolve the solid, and then slowly cooled down to room temperature at −2 °C·hr−1.
Method: Single crystal X-ray diffraction
Description: Frames were collected using Bruker D8 Venture diffractometer equipped with a Photon 100 CMOS detector employing Mo Kα radiation (λ=0.71073 Å).
Crystal system: monoclinic
| a: | 7.7688 (±0.0003) Å |
| b: | 8.5108 (±0.0004) Å |
| c: | 24.6314 (±0.0011) Å |
| α: | 90° |
| β: | 95.197 (±0.002)° |
| γ: | 90° |
Starting materials: 3-(2-ammonioethyl)anilin, PbBr2, HBr
Product: plate-like colorless crystals
Description: 0.34 mmol PbBr2, 0.35 mmol 3-(2-ammonioethyl)anilin are mixed in 3 mL of 9M HBr. The mixture is then heated to 100 ˚C for 2 h to dissolve the solid, and then slowly cooled down to room temperature at −2 °C·hr−1.
Method: Single crystal X-ray diffraction
Description: Frames were collected using Bruker D85 diffractometer at the Advanced Light Source beamline 11.3.1 (λ=0.7749 Å).
Crystal system: triclinic
| a: | 8.0135 (±0.0004) Å |
| b: | 8.427 (±0.0004) Å |
| c: | 10.7367 (±0.0005) Å |
| α: | 78.957 (±0.002)° |
| β: | 69.565 (±0.002)° |
| γ: | 89.542 (±0.001)° |
Starting materials: butanediamine, PbBr2, HBr
Product: plate-like colorless crystals
Description: 0.34 mmol PbBr2, 0.35 mmol butanediamine are mixed in 3 mL of 9M HBr. The mixture is then heated to 100 ˚C for 2 h to dissolve the solid, and then slowly cooled down to room temperature at −2 °C·hr−1.
Method: Single crystal X-ray diffraction
Description: Frames were collected using Bruker D8 Venture diffractometer equipped with a Photon 100 CMOS detector employing Mo Kα radiation (λ=0.71073 Å).
See all entries for this property (3 total)
Crystal system: monoclinic
| a: | 10.5412 (±0.0013) Å |
| b: | 11.5023 (±0.0014) Å |
| c: | 11.925 (±0.0014) Å |
| α: | 90° |
| β: | 109.996 (±0.003)° |
| γ: | 90° |
Starting materials: Histamine, PbBr2, HBr
Product: plate-like yellow crystals
Description: 0.34 mmol PbBr2, 0.35 mmol histamine are mixed in 3 mL of 9M HBr. The mixture is then heated to 100 ˚C for 2 h to dissolve the solid, and then slowly cooled down to room temperature at −2 °C·hr−1.
Method: Single crystal X-ray diffraction
Description: Frames were collected using Bruker D8 Venture diffractometer equipped with a Photon 100 CMOS detector employing Mo Kα radiation (λ=0.71073 Å).
See all entries for this property (3 total)
Crystal system: monoclinic
| a: | 10.6055 (±0.0013) Å |
| b: | 11.6091 (±0.0014) Å |
| c: | 11.9312 (±0.0014) Å |
| α: | 90° |
| β: | 110.061 (±0.003)° |
| γ: | 90° |
Starting materials: Histamine, PbBr2, HBr
Product: plate-like yellow crystals
Description: 0.34 mmol PbBr2, 0.35 mmol histamine are mixed in 3 mL of 9M HBr. The mixture is then heated to 100 ˚C for 2 h to dissolve the solid, and then slowly cooled down to room temperature at −2 °C·hr−1.
Method: Single crystal X-ray diffraction
Description: Frames were collected using Bruker D8 Venture diffractometer equipped with a Photon 100 CMOS detector employing Mo Kα radiation (λ=0.71073 Å).