M. Braun and W. Frey, Crystal structure of bis(benzylammonium) lead tetrachloride,(C7H7NH3)2PbCl4, Zeitschrift für Kristallographie - New Crystal Structures 214, 331‑332 (1999). doi: 10.1515/ncrs-1999-0318.
Bis(phenylmethylammonium) lead chloride: atomic structure Verified

See all entries for this property (2 total)

Origin: experimental (T = 293.0 K)
Space group: C m c 2₁
Lattice parameters

Crystal system: orthorhombic

a:33.619 (±0.007) Å
b:7.82 (±0.001) Å
c:7.728 (±0.001) Å
α:90°
β:90°
γ:90°
Fixed parameters:
  • temperature = 293.0 K
M. Braun and W. Frey, Crystal structure of bis(benzylammonium) lead tetrachloride,(C7H7NH3)2PbCl4, Zeitschrift für Kristallographie - New Crystal Structures 214, 331‑332 (1999). doi: 10.1515/ncrs-1999-0318.
System description
Dimensionality: D
Sample type: single crystal

Starting materials: Lead chloride, benzylamine (Merck), HCl, DMF

Product: Colorless crystals

Description: Benzyl ammonium chloride was prepared by adding a stoichiometric amount of 37% concentrated HCl to benzylamine. Then, the solvent from a dimethylformamide solution of lead chloride and benzyl ammonium chloride (1:2) was slowly evaporated.

Method: Single crystal X-ray diffraction

Description: Nicolet P3, Wyckoff diffractometer with Mo Ka radiation (0.71073 À)

Extraction method: Manual entry
Entry added on: April 15, 2019, 9:54 p.m.
Entry added by: Xiaochen Du Duke University
Last updated on: June 22, 2022, 10:12 p.m.
Last updated by: Rayan C Duke University
Data correctness verified by:
  • Rayan C Duke University

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